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NMR/EPR Spectrometers
Location: Brown 353A
Console
- AVANCE NEO, four TRX channels
Magnet
- Bruker Ascend 800 MHz/54mm bore
Probes
- 5mm Inverse Triple Resonance (TXI) probe
- Inner coil for 1H observation
- Outer coils for decoupling 13C and 15N nuclei
- Equipped with an Automatic Tuning and Matching Accessory (ATMA)
- 5mm TCI 1H & 19F CryoProbe
- Triple resonance inverse probe for 1H observe and simultaneous 13C and 15N decoupling. 1H coil is tunable to 19F.
Accessories
- GAB/2 XYZ-axis Gradient Amplifiers
- Automatic 24 sample automatic carousel
- Precooling and stabilization accessory (BCU II) for ultra-precise low temperature control from near ambient conditions down to -40 °C sample temperature ideal for biopolymers.
The Bruker AVANCE NEO-800 NMR Spectrometer was acquired through the support of New York University.
Location: Brown 353A
The 800 MHz Bruker Avance NEO NMR system is capable of performing magic angle spinning solid-state NMR experiments using our modular Phoenix 1.6 mm Quadruple Resonance (HFXY) MAS probe.
Capabilities:
- 1.6 mm sample rotor (8 uL active sample)
- Sample rotation between 8,000 and 40,000 Hz
- Multiple channel configurations:
- Quadrupole Resonance Mode:
H Channel: 1H and 19F X Channel: 31P to 13C Y Channel: 23Na to 15N
- Triple Resonance Modes:
H Channel: 19F X Channel: 31P to 13C Y Channel: 23Na to 15N
H Channel: 1H X Channel: 31P to 13C Y Channel: 23Na to 15N
H Channel: 1H and 19F X Channel: 31P to 15N
- Double Resonance Modes:
H Channel: 1H and 19F
H Channel: 1H X Channel: 31P to 13C
H Channel: 19F X Channel: 31P to 13C
- Dedicated 2H lock channel for Bio-SSNMR studies
- Variable temperature range between -125 °C to +125 °C
The Phoenix Solid-State NMR Probe was acquired through the support of New York University.
Location: Brown 353A
Console
- AVANCE III, three RF channels
Magnet
- Bruker Ascend 600 MHz/54mm bore
Probes
- 5mm Inverse Quadrauple Resonance (QXI) probe
- Inner coil for 1H observation
- Outer coils for decoupling 13C, 15N and 31P nuclei
- Equipped with an Automatic Tuning and Matching Accessory (ATMA)
- 5mm Broadband Fluorine Observe Smart (BBFO) probe
- Inner coil for broadband nuclei detection from 109Ag to 31P
- Outer coil for 1H decoupling
- Equipped with an Automatic Tuning and Matching Accessory (ATMA)
- 5mm TCI CryoProbe
- Triple resonance inverse probe for 1H observe and simultaneous 13C and 15N decoupling
Accessories
- GRASP II Z-axis Gradient Spectroscopy accessory
- Precooling and stabilization accessory (BCU1) for ultra-precise low temperature control from near ambient conditions down to 0 °C sample temperature ideal for biopolymers.
The Bruker AVANCE III-600 NMR Spectrometer was acquired through the support of New York University.
The CPTCI-cryoprobehead was acquired through the support of the National Institute of Health S10 grant under Award Number OD016343.
Location: Brown 353A
Console
- AVANCE NEO, three TRX channels
Magnet
- Bruker UltraShield 500 MHz/54mm bore
Probes
- 5mm X-Optimized Double Resonance Cryo Probe
- Broadband nuclei from 15N to 31P and 19F
- 1H observe/ X-nuclei decoupling capable
- X-nuclei observe / 1H decoupling capable
- Z axis gradient with 5 G/A*cm
- Equipped with an Automatic Tuning and Matching Accessory (ATMA)
Accessories
- Precooling and stabilization accessory (BCU I) for low temperature control from near ambient conditions down to ~0 °C sample temperature.
This instrument is accessible to all chemistry research groups except every Thursday morning between 9:00 and 10:30 am (for liquid Nitrogen/Helium filling).
The Bruker Avance NEO 500 NMR Spectrometer was acquired through the support of New York University.
Location: Brown 353A
Console
- AVANCE, dual channel
Magnet
- Bruker UltraShield 400 MHz/54mm bore
Probes
- 5mm Multinuclear broadband observe (BBO) probe
- Inner coil tuning range from 15N to 31P nuclei
- Outer coil can be tuned to 1H
- Equipped with an Automatic Tuning and Matching Accessory (ATMA)
- 5mm Inverse 1H/13C SEI probe
Accessories
- GRASP II Gradient Spectroscopy accessory
- A low temperature accessories, for operation down to -100 °C: 25 liter nitrogen dewar, nitrogen evaporator, and insulated transfer line.
This instrument is accessible to all chemistry research groups except every Thursday morning between 9:00 and 10:30 am (for liquid Nitrogen/Helium filling).
The Bruker Avance-400 NMR Spectrometer was acquired through the support of the National Science Foundation under Award Number CHE-01162222.
Location: Brown 252
Console
- AVANCE III, two RF channels
Magnet
- Bruker Ascend 400 MHz/54mm bore
Probes
- 5mm Broadband Fluorine Observe Smart (BBFO) probe
- Inner coil for broadband detection from 15N to 31P and 19F
- Outer coil for 1H decoupling
- Equipped with an Automatic Tuning and Matching Accessory (ATMA)
Accessories
- GREAT 3/10 XYZ Gradient Amplifier
During office hours from 9 am to 5 pm the maximum sign up time is an hour to ensure everyone has the access, teaching labs use are excluded from this restriction and have priority
The Bruker AVANCE III-400 NMR Spectrometer was acquired through the support of New York University.
Location: Silver 714
Console
- AVANCE III HD, two RF channels
Magnet
- Bruker Ascend 400 MHz/54mm bore
Probes
- 5mm X-nuclei-optimized CryoProbe
- Inner coil optimized to observe nuclei from 15N to 31P, with the excluded region from 199Hg to 153Eu
- Outer coil for 1H decoupling
- Equipped with an Automatic Tuning and Matching Accessory (ATMA)
- 5mm Broadband Fluorine Observe Smart (BBFO) probe
- Inner coil for broadband detection from 15N to 31P and 19F
- Outer coil for 1H decoupling
- Equipped with an Automatic Tuning and Matching Accessory (ATMA)
Accessories
- GRASP II Z-axis Gradient Spectroscopy accessory
The Bruker AVANCE III HD-400 NMR Spectrometer was acquired through the support of New York University.
Location: Waverly 968
Console
- ELEXSYS E500
- SuperX FT-EPR Microwave Bridge
Magnet
- 10 inch double yoke magnet
- 12 kW solid-state power supply
Resonators
- ELEXSYS Super High Sensitivity probehead
- ER4116DM Dual mode resonator for parallel mode experiments
- ER4118X-MS-5W Flexline Splitring for transient experiments
Accessories
- Cryogen-free Stinger System for variable temperature experiments.
Sample temperature range from ~5 to 250 K
- ER4118CF-O VT Cryostat for the Flexline resonator
- ER4112HV-11 Cryostat for high sensitivity and dual mode resonantors
- UV irradiation system with a 100W Hg lamp, shutter, light chopper and 400-700 nm band-pass filter accessories
The Bruker ELEXSYS E500 EPR Spectrometer was acquired through the support of the National Science Foundation-Major Research Instrumentation Program and New York University.